Data for 2018/2019
Analytical Chemistry II
Credits | 4 |
Hours per week | 2 / 1 / 0 |
Examination | C+Ex |
Study Language | English |
Level | Bachelor subject |
Guarantor |
doc. RNDr. Ing. Pavel Řezanka, Ph.D. doc. Ing. Kamil Záruba, Ph.D. |
Supplemental electronic materials | available at UCT Prague's e-learning |
Summary
Lectures of Analytical Chemistry II extend and complement the basic overview of the methods discussed in the course Analytical Chemistry I. They focus primarily on understanding the principles of modern methods of instrumental analysis. The exercises are divided into two sections. The first involves the uncertainty of the quantitative analysis, the other is focused on the foundations of structural analysis - infrared spectrometry, proton NMR spectrometry, and mass spectrometry spectra will be solved.
Syllabus
1. Uncertainties and testing of hypotheses in analytical chemistry
2. Vibrational spectrometry - reflection IR, IR microscopy, NIR spectrometry, Raman spectrometry
3. NMR spectrometry - relaxation, chemical exchange, NMR imaging
4. Enhanced mass spectrometry
5. Hyphenated techniques 1 - GC-MS, LC-MS, CE-MS
6. Hyphenated techniques 2 - GC/LC-ICP-MS, speciation analysis; LC/GC-IR, LC-NMR
7. Surface analysis 1 - by photons, electrons, ions
8. Surface analysis 2 - by a probe (STM, AFM, SNOM)
9. Analysis of chiral compounds - Introduction to chiral separation and chiroptic methods
10. Kinetic methods of analysis
11. Radioanalytical methods
12. Biochemical analysis
13. Chemical sensors and biosensors
14. Process analysis
2. Vibrational spectrometry - reflection IR, IR microscopy, NIR spectrometry, Raman spectrometry
3. NMR spectrometry - relaxation, chemical exchange, NMR imaging
4. Enhanced mass spectrometry
5. Hyphenated techniques 1 - GC-MS, LC-MS, CE-MS
6. Hyphenated techniques 2 - GC/LC-ICP-MS, speciation analysis; LC/GC-IR, LC-NMR
7. Surface analysis 1 - by photons, electrons, ions
8. Surface analysis 2 - by a probe (STM, AFM, SNOM)
9. Analysis of chiral compounds - Introduction to chiral separation and chiroptic methods
10. Kinetic methods of analysis
11. Radioanalytical methods
12. Biochemical analysis
13. Chemical sensors and biosensors
14. Process analysis
Literature
1. PDFs of lectures
2. Skoog, Holler, Nieman, Principles of Instrumental Analysis, Brooks/Cole Thomson Learning
3. Skoog, West, Holler, Crouch, Fundamentals of Analytical Chemistry, Brooks/Cole Thomson Learning
2. Skoog, Holler, Nieman, Principles of Instrumental Analysis, Brooks/Cole Thomson Learning
3. Skoog, West, Holler, Crouch, Fundamentals of Analytical Chemistry, Brooks/Cole Thomson Learning